Alexandria Digital Research Library

X-Band EPR Spectrometer with Customizable Arbitrary Waveform Generator based on a 1 GHz DAC Board

Author:
Kaufmann, Thomas
Degree Grantor:
University of California, Santa Barbara. Chemistry
Degree Supervisor:
Songi Han
Place of Publication:
[Santa Barbara, Calif.]
Publisher:
University of California, Santa Barbara
Creation Date:
2012
Issued Date:
2012
Topics:
Chemistry, General, Chemistry, Physical, and Physics, General
Keywords:
Magnetic Resonance
Electron Paramagnetic Resonance
Pulse Shaping
AWG
Arbitrary Waveform Generation
EPR
Genres:
Online resources and Dissertations, Academic
Dissertation:
M.S.--University of California, Santa Barbara, 2012
Description:

We present an electron paramagnetic resonance (EPR) spectrometer featuring an arbitrary waveform generator (AWG) operating at 8--10 GHz (X-band) and based on a 1 GHz digital-to-analog converter (DAC) board with a 42 dB (i.e. 14-bit) dynamic range, which was developed to widen the scope of pulsed EPR and enable new experiments. This spectrometer generates shaped pulses with precise amplitude and phase control and can specify pulse lengths and delays with a time resolution of ≤250 ps. We demonstrate the capabilities of the spectrometer by presenting spin-echo measurements that implement an entirely digitally controlled and calibrated 16-step phase cycle and by measuring the excitation profiles seen by the spins in the microwave resonator as they respond to various pulse shapes, including rectangular, triangular, Gaussian, sinc and adiabatic rapid passage waveforms. Potential applications of these capabilities, and their implementation in commercial instrumentation will be discussed.

Physical Description:
1 online resource (45 pages)
Format:
Text
Collection(s):
UCSB electronic theses and dissertations
ARK:
ark:/48907/f34x55sm
ISBN:
9781267939630
Catalog System Number:
990039503260203776
Rights:
Inc.icon only.dark In Copyright
Copyright Holder:
Thomas Kaufmann
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